DMF recovery process is a typical chemical distillation process, characterized by a large degree of correlation between process parameters and a high requirement for recovery indicators. From the current situation, the conventional instrument system is difficult to achieve real-time and effective monitoring of the process, so the control is often unstable and the composition exceeds the standard, which affects the production efficiency of enterprises. For this reason, our company and Beijing University of Chemical Technology jointly developed THE DCS control system of DMF recycling engineering computer.